Particle Size by Insitu Impactor

This in-stack analysis can be done by Clean Air's Testing Services or you can choose to rent the necessary equipment. The applicable phone numbers are listed towards the bottom of these pages.

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In this method, particulate matter is withdrawn under isokinetic conditions and segregated by size in an cascade impactor. The Andersen Mark III cascade impactor uses the principle of inertial separation to size segregate particulate samples from the gas stream. The impactor has eight stages for particle size determination. Each stage gives a cut-point based on aerodynamic diameter of the particle.

Aerodynamic diameter is defined as the diameter of a sphere of unit density ( 1 g/cm3 ) that attains the same terminal settling velocity (vs) at a low Reynolds number as the actual particle under consideration. For mathematical modeling purposes, it is convenient to express the behavior of an irregularly shaped particulate specimen as if it were a spherical particle. Use of such common denominators makes it easier to predict, compare and correlate various materials. The Stokesian, or Equivalent, Diameter is the diameter of a sphere having the same terminal settling velocity and density as the particle under consideration. Typically, the density of a particulate sample is not known during field sampling. All calculations in the field are therefore performed assuming unit particle density ( 1 g/cm3 ).

During sampling, the particles are driven (jetted) toward a collecting surface where they may cling. By changing the velocity (orifice size of the jet), the size of the particles collected is controlled. The size of the jets within each stage is constant, but for each succeeding stage the jets get smaller. Impaction occurs when the particle's inertia overcomes the aerodynamic drag. Otherwise, the particle remains in the air stream and proceeds to the next stage. To keep the cut-point for each stage constant, the impactor must be operated at a constant flow rate. At each stage, the particle impacts on a desiccated, tared, Whatman 934AH glass fiber mat. Following sampling, the samples are cooled in a desiccator and weighed to 0.00001g.

Test time for particle size distribution is dependent on the actual grain loading of the gas stream. The following definitions are given to aid in the understanding of sampling methodology and data interpretation.

Reynolds Number (Orifice Flow)
The Reynolds number is a dimensionless quantity that establishes the proportionality between fluid inertia and the sheer stress due to viscosity. It's significance in this application is that it can be used to determine whether or not the flow through the orifice was laminar or turbulent. One strives to avoid turbulence within the impactor as this could disturb the particulate on the individual stages. As a general rule of thumb, Reynolds numbers greater than 4000 represent totally turbulent conditions, whereas values in the range of 1000 to 2000 represent laminar flow. In the region between these two values, the flow contains both laminar and turbulent components.

Cut Diameter (D50) of Various Particle Sizes
Cut diameter is calculated for each stage. It is the particle diameter for which the efficiency and the penetration is 50% or where half these size particles are captured and half penetrate the collector.

Reynolds Number (Particle)
This quantity is a dimensionless number used to characterize the movement of a particle in a system where the containing walls have essentially no effect on the motion of the particle (as is the case in an ESP). During impactor data reduction, the terminal setting velocity of the particles must be calculated. This velocity is used to determine the first stage cut diameter (D50). These calculations involve a dimensionless drag coefficient (often called the particle friction factor) which is dependent on the particle Reynolds number.

Knudsen Number (Particle)
This dimensionless number is used to indicate how far a gaseous system (including the particles) deviates from a continuous system. When this value is less than 0.1 (larger particles), the gas flow is in the continuum regime and one set of equations are used to obtain velocity. When the Knudsen number is between 0.1 and 1 (smaller particles), the gas flow is considered to be in the slip flow regime and a correction to the equations for the continuum regime is used when calculating velocity. With slip flow, the particle appears to "slip through" the gas molecules.

dM/dlogD
This is the differential particle size distribution. It assumes that all mass captured on a given stage in the impactor consists of material with diameters greater than the D50 of that stage and less than the D50 of the previous stage. Since the intervals between these D50s are logarithmically related, the change in mass (dM) divided by the change in size (dlogD) gives an approximation of the amount of material contained in that size band. By comparing these values for inlet and outlet test runs, fractional efficiencies (efficiencies for given size bands) for the pollution control device can be easily obtained.

Geometric Mean Diameter
Most aerosols (e.g., fly ash in flue gas) have particle size distribution that are approximately log-normal. That is, they have a bell-shaped curve if the number of particles of a given size are plotted as a function of the logarithm of their diameter. The diameter corresponding to the center of the bell-shaped curve for this distribution is called the geometric mean diameter. In addition, a geometric mean diameter can be calculated for each size band of the differential size distribution (see above). These individual diameters are then used to plot each value of dM/dlogD (for a given impactor stage) as a function of the logarithm of the geometric mean for that size interval.

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Particle Size using a Anderson Mark III Cascade Impactor

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