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Overview
Air Quality Consulting / Management
Analytical Services
Chromatography and Wet Methods
Coating and Ink Analysis
ESP Modeling
Flue Gas Desulfurization System Sample Analyses
Flyash Analysis
Gravimetric Analysis
Inorganic Analysis
Organic Analysis
Particle Characterization
Resistivity Analysis
Resistivity and Particle Size Introduction
Function of Temperature
Fig. 1: Temp. vs. Resistivity
Resistivity in Simulated Flue Gas
Table 1: Coal and Ash Chemistry
Fig. 2: Resistivity vs. Electric Field
Fig. 3: Resistivity Model
Particle Size Distribution
Fig. 4: Bahco Particle Size
Greenhouse Gas Management
Mercury Monitoring
Performance / Efficiency
Performance Test Instrumentation Support
Stack / Source Emissions Testing

 

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Price Schedule

Fee schedule for analytical work performed at Clean Air Engineering Laboratories:

Organic Compound Analysis

Laboratory Resistivity Determinations*

Coating and Ink Analysis

Computer Model ESP Performance Predictions

Inorganic Analysis

Rush Analysis Pricing

Gravimetric Analysis

 

Organic Compound Analysis
Clean Air Engineering's organic laboratory specializes in the analysis of samples collected from source and ambient test programs. Clean Air utilizes gas chromatographs manufactured by Hewlett Packard, Perkin Elmer and MTI coupled with flame ionization, flame photometric and thermal conductivity detectors. Clean Air requires that all analysis be pre-approved before sending samples to verify that the analysis objectives can be achieved. The price schedule for organic analysis per sample is as follows:

 

First Compound

Each Additional Compound

Adsorbent Tube

$100/sample

$60/sample

Impinger Catch

$80/sample

$50/sample

Tedlar Bag

$80/sample

$50/sample



Coating and Ink Analysis

EPA Method 24

$250/sample

Clean Air Engineering's organic laboratory regularly performs EPA Method 204a analyses on liquid coating and ink samples. Results of this analysis include: 1) A direct comparison of FID Response Factor from the coating with propane calibration gas; 2) Determination of VOC Content of the liquid sample.

EPA Method 204a

$250/sample

EPA Method 204f $100/sample

Ten or More Samples

10% Discount on Analysis

Twenty or More Samples

25% Discount on Analysis




Inorganic Analysis
Clean Air Engineering's inorganic laboratory utilizes a Dionex Model DX300 ion chromatograph. All analyses are performed in accordance with procedures in US EPA Methodology. Full pre and post analyses calibrations are provided as part of the per project pricing. The price schedule for inorganic analysis is as follows:

Ion Chromatography - Cations

Instrument Set-Up, Calibration and Reporting Cost:

$250/project

Lithium:

$27/sample

Sodium:

$27/sample

Potassium:

$27/sample

Ammonium:

$27/sample

Magnesium:

$27/sample

Calcium:

$27/sample

Full Scan For All Above Cations:

$75/sample


Ion Chromatography - Anions

Instrument Set-Up, Calibration and Reporting Cost:

$250/project

Fluoride:

$27/sample

Chloride *:

$27/sample

Nitrite:

$27/sample

Bromide:

$27/sample

Nitrate:

$27/sample

Phosphate:

$27/sample

Sulfate:

$27/sample

Full Scan For All Above Anions:

$75/sample

* Please note that BIF Method 9057 for HCl/Cl2 calls for two sample analyses per run and would cost $50 per run.

Ion Chromatography - Carbonate

Instrument Set-Up and Reporting Cost:

$250/project

Carbonate:

$25/sample

Formate: $25/sample
Acetate: $25/sample
Propionate: $25/sample
Sulfate: $25/sample

Titration Analysis

Sulfur Dioxide (Method 6):

$40/sample

Sulfuric Acid Mist (Method 8):

$40/sample




Gravimetric Analysis
Clean Air Engineering's gravimetric laboratory performs analysis on particulate samples collected using federal and state test methods.

Gravimetrics - Method 5, Method 17, CARB Method 5

Front-Half Analysis

Filter:

$30/sample

Probe Wash:

$30/sample


Back-Half Condensable

Gravimetric analysis of aqueous condensable (inorganic):

$30/sample

Organic solvent extractable residue:

$50/sample

Back half acetone organic rinse (if required):

$30/sample

Back half filtration analysis:

$40/sample

Please note that some states require the additional back half filtration (such as Pennsylvania and New Jersey). If Method 202 sulfate analysis is required, ion chromatography charges will apply (see page 2).

Gravimetrics - Road Silt Determinations

Road Silt determined in accordance with EPA Report 450/3-88-008

"Procedures for Sampling Surface/Bulk Materials"

$100/sample

Tared Filter Media

8.26 cm Diameter Filters

934 AH Glass Fiber

$25 each

QAT UP Quartz Fiber

$30 each

Teflon Filter $30 each

4.7 cm Diameter Filters

934 AH Glass Fiber (double w/ gaskets)

$25 each

QAT UP Quartz Fiber

$30 each


8" x 10" (Hi-Vol Filters)

934 AH Glass Fiber

$30 each

Quat UP Quartz Fiber

$35 each


M17 Alundum Thimbles

$100 each

37mm Acetate Membrane Cassette Filter

$25 each

Note: Post weights are all $15 each

Rinses: Acetone and DI H20 $30 each; MeCL extract $50 each



Laboratory Resistivity Determinations*
Laboratory resistivity and particle size analysis of particulate can be determined to aid in improving control device performance. Clean Air determines resistivity as a function of temperature in accordance with IEEE Standard 548. Particle size is determined using the Bahco Micro Particle Classifier.

IEEE Standard 548-1984

Round Trip - Resistivity measured as a function of ascending and descending test temperature between 85°C and 450°C in an environment of air containing one specified water concentration at an average electric field intensity of 4kV/cm

$1,000 sample

  

Ascending temperatures only; otherwise same as round trip:

$850 sample

  

Descending temperatures only; otherwise same as round trip:

$600 sample

  

Descending temperatures with one ascending data point at the temperature of principal interest; otherwise same as round trip:

$725 sample

 

Resistivity as a function of applied electric field at a specified temperature:

$650 sample


With Sulfuric Acid or Ammonia Environment; EPA Report 600/7-78-035

Single point determination - Resistivity measured isothermally as a function of electric field intensity in an environment of air containing a specified concentration of water and sulfuric acid or ammonia vapor (48 hour test)

$1,000 sample

  

Each additional data point produced by changing temperature, water concentration, sulfuric acid vapor concentration or ammonia vapor concentration (24 hour test):

$600 sample


Computer Model Resistivity Predictions

Resistivity predicted as a function of temperature and environmental conditions (water and sulfuric acid concentration) using customer-supplied coal and ash compositional data. Model II described in EPA-600/7-86-010 is used; with brief comment

$250/sample

Predicted inherent and sodium-depleted volume resistivity using customer-supplied ash compositional data. Described in EPRI Report CS-3421; with brief comment:

$250/sample



Computer Model ESP Performance Predictions
Particle collection performance of an electrostatic precipitator is predicted using customer-supplied precipitator mechanical and electrical data as well as coal and fly ash compositional data. Model is described in EPA-600/7-84-069 a&b and is commonly referred to as the EPA/SRI computer model. In addition to modeling the existing precipitator performance, the effects of various changes (such as coal switching and gas conditioning) can be predicted. Priced according to scope and complexity.

Other Services

Bahco particle size classification with density correction

$300/sample

Ash mineral analysis and loss-on-ignition (LOI)

$350/sample

Short proximate, ultimate coal analysis

$150/sample

Soluble sulfate analysis on ash

$50/sample

Sieve analysis

$75/sample


Scanning electron microscopy (SEM), x-ray diffraction, designed resistivity tests, and consultation work are available and are priced according to scope and complexity.

Rush Analysis Pricing
Analytical results will be issued 15 working days from the receipt of samples. Rush analytical results may be available at increased rates upon request. Rush charges for analysis will be applied in the following manner:

1-2 working days

300% of listed price

3-5 working days

200% of listed price

6-10 working days

150% of listed price

In any circumstance, a purchaser's request for rush analysis in a certain time frame authorizes all degrees of rush charges up to that extent. Rush charges on the final invoice will be reflective of when results were available and reported to the Purchaser. All days will be calculated on a five day work week (with allowance for holidays).

All analyses will be performed according to Clean Air Engineering's
Terms and Conditions for Laboratory Work.

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500 W. Wood Street
Palatine, IL 60067, USA
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